Tag Archives: 0352-0080

Mobile Phase and Reagents for Paralytic Shellfish Toxins Analysis

Overview

Shellfish variations imageMobile Phase and Reagents for Paralytic Shellfish Toxins Analysis

For Post-Column Analysis Using Fluorescence Detector

Some species of microscopic algae produce naturally occurring toxin referred to as biotoxin. Under certain water conditions, they “bloom” and produce high concentrations of the biotoxin. Paralytic shellfish toxins are biotoxins produced by the dinoflagellates and these toxins can concentrate in shellfish. Since the ingestion of contaminated shellfish can lead to paralytic shellfish poisoning, a life-threatening illness, the shellfish population should be regularly monitored for these toxins.

An HPLC method that utilizes post-column oxidation of the toxins under acidic conditions has been approved as a new official AOAC method – OMA 2011.02. Three groups of toxins are separated on a C18 column using a single step-gradient method. The products of post-column derivatization of the toxins can be detected with high sensitivity using a fluorescence detector. This can be carried out very easily using any HPLC (with quaternary pump), Pickering post-column instrument (Vector PCX or Onyx PCX), and Pickering Lab’s newest mobile phases and reagents.

 

 

Pricing & Ordering

 

Pricing & Ordering

Mobile Phase and Reagents for Paralytic Shellfish Toxins AnalysisLogin for Prices

Catalog #

Description

Quantity

PSP-0001

GTX & STX Mobile Phase A, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-0002

GTX & STX Mobile Phase B, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-C003

C-Toxins Mobile Phase A, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-C004

C-Toxins Mobile Phase B, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-R1

PSP Two-part Post-column Oxidant, to prepare case of 4 (950 mL/bottle)

each

PSP-R2

PSP Post-column Acid, each (950 mL/bottle)

each


 

 

 

 

 

 

Food & Supplement Testing: Post-column Analysis Kits

Food & Supplement Testing:

Post-column Analysis Kits 

 
BIOGENIC AMINES/POLYAMINES ANALYSIS KIT:Login for Prices

Catalog #

Description

Quantity

0352-0040

Biogenic Amines/Polyamines Analysis Kit:

each

9410917

ALKION™ Cation-exchange Column, K form, 4.0 × 150 mm

each

9493020

ALKION™ Guard Column, K+ form, 3.0 × 20 mm

each

1100-0161

Flow Restrictor, PEEK Tubing, 0.005" ID, 550 psi @ 0.3 mL/min in 15% Methanol in Water. (Replacement for 1100-0200, OPA Flow Restrictor)

each

K563

Potassium Phosphate Eluant, pH 5.63, 4 × 950 mL

each

K600

Potassium Phosphate Eluant, pH 6.00, 4 × 950 mL

each

K130

Potassium Column Regenerant, 950 mL

each

OD104

OPA Diluent, 4 × 950 mL

case of 4 x 950 mL/bottle

O120

o-Phthalaldehyde, 5 g

each (5 g/bottle)

3700-2000

Thiofluor™, 10 g

each (10 g/bottle)


   
  
 
AMINOGLYCOSIDE ANTIBIOTICS ANALYSIS KIT:Login for Prices

Catalog #

Description

Quantity

0352-0041

Aminoglycoside Antibiotics Analysis Kit:

each

9410917

ALKION™ Cation-exchange Column, K form, 4.0 × 150 mm

each

9493020

ALKION™ Guard Column, K+ form, 3.0 × 20 mm

each

1100-0161

Flow Restrictor, PEEK Tubing, 0.005" ID, 550 psi @ 0.3 mL/min in 15% Methanol in Water. (Replacement for 1100-0200, OPA Flow Restrictor)

each

1700-1101

Potassium Phosphate Eluant, KO1, 4 × 950 mL

each

1700-1102

Potassium Hydroxide Eluant, KO2, 4 × 950 mL

each

1700-1103

Potassium Chloride Eluant, KO3, 4 × 950 mL

each

OD104

OPA Diluent, 4 × 950 mL

case of 4 x 950 mL/bottle

O120

o-Phthalaldehyde, 5 g

each (5 g/bottle)

3700-2000

Thiofluor™, 10 g

each (10 g/bottle)


   
  

MULTI-RESIDUE MYCOTOXIN KIT:Login for Prices

Catalog #

Description

Quantity

0352-0053

MULTI-RESIDUE MYCOTOXIN KIT :

each

1612124

MYCOTOX™ Reversed-phase Column, 4.6 × 250 mm

each

3106-0578

Reverse Phase Guard Holder with 3 cartridges 4.3mm

each

OD104

OPA Diluent, 4 × 950 mL

case of 4 x 950 mL/bottle

O120

o-Phthalaldehyde, 5 g

each (5 g/bottle)

1700-1108

Sodium Phosphate Eluant, pH 3.3, 4 x 950 mL

each

3700-2000

Thiofluor™, 10 g

each (10 g/bottle)


   
  
  
AFLATOXINS ANALYSIS KIT:Login for Prices

Catalog #

Description

Quantity

0352-0050

Aflatoxin Analysis Kit:

each

1612124

MYCOTOX™ Reversed-phase Column, 4.6 × 250 mm

each

3106-0578

Reverse Phase Guard Holder with 3 cartridges 4.3mm

each


 
    
POLYETHER ANTIBIOTICS KIT:Login for Prices

Catalog #

Description

Quantity

0352-0051

Polyether Antibiotics Kit:

each

2381750

Polyether Column, 4.6 × 250 mm

each

3106-0578

Reverse Phase Guard Holder with 3 cartridges 4.3mm

each

3700-2200

Vanillin, 30 g

each (30 g/bottle)

 
    

PARALYTIC SHELLFISH TOXINS ANALYSIS KIT:Login for Prices

Catalog #

Description

Quantity

0352-0080

Paralytic Shellfish Toxins Analysis Kit:

each

PSP-0001

GTX & STX Mobile Phase A, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-0002

GTX & STX Mobile Phase B, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-C003

C-Toxins Mobile Phase A, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-C004

C-Toxins Mobile Phase B, case of 4 (950 mL/bottle)

case of 4 (950 mL/bottle)

PSP-R1

PSP Two-part Post-column Oxidant, to prepare case of 4 (950 mL/bottle)

each

PSP-R2

PSP Post-column Acid, each (950 mL/bottle)

each